From: Yaritza Brinker <YBrinker**At_Symbol_Here**FELE.COM>
Subject: Re: [DCHAS-L] Acid and Base (glass wash) Bath Containers
Date: Fri, 10 Jan 2020 20:01:26 +0000
Reply-To: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**PRINCETON.EDU>
Message-ID: BN8PR05MB649893A8764B3DB532F69266AD380**At_Symbol_Here**BN8PR05MB6498.namprd05.prod.outlook.com
In-Reply-To


My experience with dipping baskets in general, is that they work great for items that don't hold water. Items that do hold water require a bit of care not to spill, but should work just fine.

If you decide to go with a standard bucket without markings, don't forget to add some sort of "max fill line" to the bucket. Otherwise, the fluid coming out of the holes can spill out because people don't always lift the basket slowly enough to prevent that.

Thank you,

Yaritza Brinker
260.827.5402

-----Original Message-----
From: ACS Division of Chemical Health and Safety On Behalf Of Monique Wilhelm
Sent: Thursday, January 9, 2020 6:00 PM
To: DCHAS-L**At_Symbol_Here**PRINCETON.EDU
Subject: Re: [DCHAS-L] Acid and Base (glass wash) Bath Containers

** External Email **

Has anyone used this 5 gallon bucket with dipping basket combination?
If so, what was your experience?

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Monique

_________________________________________________________

Monique Wilhelm, M.S., NRCC Certified CHO

ACS CHAS Secretary|2017 CERM E. Ann Nalley Award Recipient

Laboratory Manager|Adjunct Lecturer|Chemistry Club Advisor

Department of Chemistry & Biochemistry|University of Michigan-Flint


Monique

_________________________________________________________

Monique Wilhelm, M.S., NRCC Certified CHO

ACS CHAS Secretary|2017 CERM E. Ann Nalley Award Recipient

Laboratory Manager|Adjunct Lecturer|Chemistry Club Advisor

Department of Chemistry & Biochemistry|University of Michigan-Flint


On Mon, Dec 2, 2019 at 6:30 PM Janice Umbaugh wrote:
>
> Kimi,
>
>
>
> The style of tank that was recommended is only good if the baths aren‰??t being moved. We use similar style round tanks for manufacturing, and even with the lip to keep splashes from escaping, they aren‰??t safe to be moved if they‰??re over half full. You can buy them with spigots, though, and that makes them easier to empty and clean. The spigots are likely a source of leaks, though, and can be knocked off fairly easily.
>
>
>
> As far as the buckets with lids go, watch out for the gaskets in the lids. Depending on the kind of gasket, the material in the bath can degrade the gasket and keep the buckets from sealing properly. I like the containment buckets that are used to overpack returns of hazardous materials. The larger ones have handles molded in and locking lids.
>
>
>
> Thanks,
>
> Janice Umbaugh
>
>
>
>
>
> From: ACS Division of Chemical Health and Safety
> [mailto:DCHAS-L**At_Symbol_Here**PRINCETON.EDU] On Behalf Of Yaritza Brinker
> Sent: Monday, December 02, 2019 5:13 PM
> To: DCHAS-L**At_Symbol_Here**PRINCETON.EDU
> Subject: Re: [DCHAS-L] Acid and Base (glass wash) Bath Containers
>
>
>
> In my experience, 5gal buckets of KOH cleaner are bad news. People don‰??t necessarily respect the bucket and they don‰??t cap it well. You end-up with KOH all over the floor from people taking their parts/glassware out. Every once in a while, you‰??ll get someone deciding to move the bucket‰?| and spill it in the process because it wasn‰??t capped well.
>
>
>
> If possible, you might want to consider using an Alconox product or something similar in lieu of the KOH bath. Alconox makes several different glassware cleaning products that clean up most of the residues out there. I‰??ve used these products with good results.
>
>
>
> If you have to continue to use baths, I‰??d suggest you take a page off the parts washers‰?? book.
>
> Cleaning the tank can be a challenge with tanks larger than 1 or 2 gallons. Thus, larger parts cleaners usually have their own stand/cart and have a drain hose.
>
> Location can be an issue. If it‰??s on the counter, you‰??ll need to consider ergonomics so the tank is not too high up.
>
> Also, you need to consider the weight of the full tank‰?| ~8lbs/gal of water. So, even a 5gal bucket filled å1Ú2 way will weigh about 20lbs. It doesn‰??t sound like much, but that is the same as lifting 2 large potato bags with one hand.
>
>
>
> I‰??m all for cheap problem solvers, but I‰??ve been there‰?| having to clean up the spilled 5gal bucket.
>
>
>
> Thank you,
>
>
>
> Yaritza Brinker
>
> 260.827.5402
>
>
>
> From: ACS Division of Chemical Health and Safety
> On Behalf Of Brown, Kimberly Jean
> Sent: Monday, December 2, 2019 2:44 PM
> To: DCHAS-L**At_Symbol_Here**PRINCETON.EDU
> Subject: [DCHAS-L] Acid and Base (glass wash) Bath Containers
>
>
>
> ** External Email **
>
> Hello, and Happy December!
>
>
>
> Have any of you issued (or been subject to) specific guidance regarding lab-scale acid and bath baths for glassware cleaning?
>
>
>
> After some recent spills, we evaluated the types of containers being used for acid and base baths in our labs. Some groups are using 5-gallon buckets with poorly fitting lids, which is what led to the spills. In updating our recommendations, however, we questioned whether or not the lids should be tight-fitting (liquid/gas tight) due to the potential for pressurization.
>
>
>
> Ultimately, we recommended a product such as this: https://nam12.safelinks.protection.outlook.com/?url=https%3A%2F%2Fwww.calpaclab.com%2Fnalgene-rectangular-tank-with-cover-pp-7-gal-12x12x12%2Fng-14200-0010%23&data=02%7C01%7C%7C9f7fa3c5042d4bca3eae08d79559d2e1%7C994c3e8bb42845fb8640593ef0303f7f%7C0%7C0%7C637142085341843116&sdata=609i11gat%2BraAYjXEt6W%2BXvcE159sHcoi1jt20BYqt8%3D&reserved=0 (Which more than a few groups resisted/rejected for a variety of reasons).
>
>
>
> A researcher argued that there is no potential for pressurization of a base bath (e.g. KOH and IPA) during glassware soaking, and therefore, a bucket with a screw top lid should still be an acceptable option.
>
>
>
> Thoughts? Is there a potential for pressurization of the base bath? What requirements, if any, do you have for this?
>
>
>
> Thanks for sharing your experiences and opinions!
>
>
>
> Kimi Brown
>
> (Kimi Bush) (she, her, hers)
>
> Sr. Lab Safety Specialist
>
> Environmental Health and Radiation Safety
>
> University of Pennsylvania
>
> 3160 Chestnut St., Suite 400
>
> Philadelphia, PA 19104-6287
>
> Office: 215-746-6549
>
> Voice/cell/text: 215-651-0557
>
> fax: 215-898-0140
>
>
>
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