The lab book by Szafran, Pike and Singh is the sole example I know about. This was published in 1991 (not 2008 as Amazon says - ?) and has not been updated.
http://www.wiley.com/WileyCDA/WileyTitle/productCd-0471619965.html
Two other interesting inorganic lab books (although not microscale) are:
http://www.wiley.com/WileyCDA/WileyTitle/productCd-047146483X.html
http://www.uscibooks.com/rauch.htm
Finally: an inorganic website/clearinghouse, including experiments: https://www.ionicviper.org/
Dave
David C. Finster
Professor, Department of Chemistry
University Chemical Hygiene Officer
Wittenberg University
937-327-6441
http://userpages.wittenberg.edu/dfinster/index.html
From: DCHAS-L Discussion List [mailto:dchas-l**At_Symbol_Here**MED.CORNELL.EDU] On Behalf Of Wawzyniecki Jr, Stefan
Sent: Monday, March 12, 2012 11:53 AM
To: DCHAS-L**At_Symbol_Here**MED.CORNELL.EDU
Subject: [DCHAS-L] Microscale laboratory manual/textbook
Can anyone recommend a microscale experiment chemistry text for use in first/second year inorganic labs?
-Stefan Wawzyniecki, CIH, CHM
University of Connecticut