There is a huge body of literature on making nitrating acid solutions and for safely carrying out nitrations. Bretherick is certainly the starting place, but a good search on Science Direct and SciFinder is called for. Then, before you do bench work, develop an SOP and go over it in detail with peers and SMEs.
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Recently I start working on a project involving nitration with nitric acid, does anyone has an experience with this kind of reaction ? Also we are mixing nitric acid and acetic acid and then adding the compound to be nitrate, how dangerous is the mixing of the two acids I read that they are incompatible ?
Nadejda Spassova, Ph.D
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