Safety Emporium eyewashes
Safety Emporium eyewashes

Interactive Learning Paradigms, Incorporated

DCHAS-L Discussion List Archive


From: Thomas Szabo <info**At_Symbol_Here**YOUKAYA.COM>
Subject: Re: [DCHAS-L] Best Practices Question
Date: Wed, 11 Aug 2021 15:28:07 -0700
Reply-To: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**Princeton.EDU>
Message-ID: 05BF90A0-B480-4322-9379-6E4822F135AB**At_Symbol_Here**youkaya.com
In-Reply-To


In my experience the most common mistakes are not flushing the glass setup properly with an inert gas, BOTH before hydrogen is introduced AND after the hydrogenation is complete.


Done properly, atmospheric pressure catalytic hydrogenation is one hell of a safe and simple reaction. And having nice glassware allowing monitoring of uptake volumetrically definitely helps.

Thomas Szabo, PhD

On Aug 11, 2021, at 2:48 PM, Jack Brown <orgchem1954**At_Symbol_Here**gmail.com> wrote:

=EF=BB=BF
Hello James;
There are several groups that might be interesting for you to talk to.  However, are you interested in only lab scale hydrogenations or larger scales?  And as far as methanol filtrations or is this focused on filtration after the hydrogenation is completed?
Thanks
Jack D. Brow

On Wed, Aug 11, 2021 at 2:45 PM James Kaufman <jim**At_Symbol_Here**labsafety.org> wrote:
A colleague asked me to gather your thoughts about the following inquiry.

Do you know, or do you know of someone/group I could talk to concerning industry best practices about hydrogenation/open access hydrogenation/methanol/filtration, etc.? We would like to see if there are some practices out there that we haven't considered.

Regards ... Jim

 James A. Kaufman, PhD

Founder/President Emeritus


The Laboratory Safety Institute (LSI)

A Nonprofit Educational Organization for Safety in Science, Industry, and Education

192 Worcester Street, Natick, MA 01760-2252

(O) 508-647-1900  (F) 508-647-0062  (C) 508-574-6264  Skype: labsafe; 508-401-7406 

jim**At_Symbol_Here**labsafety.org  www.labsafety.org    Teach, Learn, and Practice Science Safely





--- For more information about the DCHAS-L e-mail list, contact the Divisional membership chair at membership**At_Symbol_Here**dchas.org Follow us on Twitter **At_Symbol_Here**acsdchas
--- For more information about the DCHAS-L e-mail list, contact the Divisional membership chair at membership**At_Symbol_Here**dchas.org Follow us on Twitter **At_Symbol_Here**acsdchas

Previous post   |  Top of Page   |   Next post