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Subject: Re: [DCHAS-L] Article

Date: Jun 7, 2021 16:50 UTC

Author: Monona Rossol <0000030664c37427-dmarc-request**At_Symbol_Here**LISTS.PRINCETON.EDU>

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Subject: [DCHAS-L] alternative etchant for metal samples

Date: Jun 8, 2021 13:54 UTC

Author: Andy Glode <andy.glode**At_Symbol_Here**UNH.EDU>

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From: Monique Wilhelm <mwilhelm**At_Symbol_Here**UMICH.EDU>

Subject: Re: [DCHAS-L] benchmarking O2 monitoring with cryogen use

Date: Jun 7, 2021 17:14 UTC

Reply-To: ACS Division of Chemical Health and Safety

In-Reply-To: Re: [DCHAS-L] benchmarking O2 monitoring with cryogen use

Demystify: 

Hi Brandon,

Having never experienced a quenching event, I would be interested in knowing more about this event. Will you be presenting or writing about it in any venue in the near future?

Best,
_________________________________________________________
Monique Wilhelm
Lab Manager
CAS, Department of Chemistry & Biochemistry | The University of Michigan-Flint
303 E. Kearsley St | Room 572 MSB | Flint, MI | 48502-1950


On Wed, Jun 2, 2021 at 3:22 PM Chance, Brandon <bchance**At_Symbol_Here**mail.smu.edu> wrote:

Ellen,

After the incident at the Georgia Sperm Bank, our PD asked us to assess any spaces where a possible deficiency may occur. We basically made some assumptions involving complete dead air (we have had a number of campus-wide power outages), calculated the volume of the laboratory (or other space), and then the size of the Dewar. If the calculations showed that a 120 or 160L Dewar could displace enough oxygen to result in a low oxygen atmosphere, we installed local monitoring. This included the NMR facility, a few labs using Dewars to act as a nitrogen gas source (we do not have house nitrogen), various storage rooms, and, last but not least - the room that houses SMU Athletics' cryotherapy unit.

Frankly, as alluded to, much of this is overkill. We have had storage rooms drop down to about 19.4% when Dewars are venting as part of their pressure relief systems. We recently had an NMR quench (that is a whole other story and involves a compressed air cylinder transported too close to the magnet). Even then, during quenching, the oxygen in the NMR room never dropped below about 20%.

Regards,

Brandon S. Chance, MS, CCHO

Director of Environmental Health and Safety

Southern Methodist University

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