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Subject: Re: [DCHAS-L] singing and wind instruments indoors
Date: Saturday, July 25, 2020 at 12:54:39 PM
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Subject: Re: [DCHAS-L] Serious Explosion during Large-Scale Preparation of an Amine
Date: Sat, 25 Jul 2020 17:36:09 -0400
Author: Carmen Nitsche

From: "Reinhardt, Peter" <peter.reinhardt**At_Symbol_Here**YALE.EDU>
Subject: [DCHAS-L] Serious Explosion during Large-Scale Preparation of an Amine
Date: Sat, 25 Jul 2020 17:10:52 +0000
Reply-To: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**Princeton.EDU>
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Peter A. Reinhardt
Director, Yale Office of Environmental Health & Safety
203-737-2123
Please see the following description of a serious incident during an Alane-based reduction of a nitrile:

 

"Serious Explosion during Large-Scale Preparation of an Amine by Alane (AlH3) Reduction of a Nitrile Bearing a CF3 Group" https://pubs.acs.org/doi/pdf/10.1021/acs.chas.0c00045

 

The article contains a number of useful points.

Please share with your research groups.

 

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