DCHAS-L Archives, Jul 25 2020 - [DCHAS-L] Serious Explosion during Large-Scale Preparation of an Amine

DCHAS-L Discussion List Archive

Previous by Date:
Subject: Re: [DCHAS-L] singing and wind instruments indoors
Date: Saturday, July 25, 2020 at 12:54:39 PM
Author: pzavon**At_Symbol_Here**ROCHESTER.RR.COM

Next by Date:
Subject: Re: [DCHAS-L] Serious Explosion during Large-Scale Preparation of an Amine
Date: Sat, 25 Jul 2020 17:36:09 -0400
Author: Carmen Nitsche

From: "Reinhardt, Peter" <peter.reinhardt**At_Symbol_Here**YALE.EDU>
Subject: [DCHAS-L] Serious Explosion during Large-Scale Preparation of an Amine
Date: Sat, 25 Jul 2020 17:10:52 +0000
Reply-To: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**Princeton.EDU>
Message-ID: BN8PR08MB628909ED84AD5F1C56289BE692740**At_Symbol_Here**BN8PR08MB6289.namprd08.prod.outlook.com
In-Reply-To

Peter A. Reinhardt

Director, Yale Office of Environmental Health & Safety

203-737-2123

Please see the following description of a serious incident during an Alane-based reduction of a nitrile:

"Serious Explosion during Large-Scale Preparation of an Amine by Alane (AlH₃) Reduction of a Nitrile Bearing a CF₃ Group" https://pubs.acs.org/doi/pdf/10.1021/acs.chas.0c00045

The article contains a number of useful points.

Please share with your research groups.

Previous post | Top of Page | Next post

The content of this page reflects the personal opinion(s) of the author(s) only, not the American Chemical Society, ILPI, Safety Emporium, or any other party. Use of any information on this page is at the reader's own risk. Unauthorized reproduction of these materials is prohibited. Send questions/comments about the archive to secretary**At_Symbol_Here**dchas.org.
The maintenance and hosting of the DCHAS-L archive is provided through the generous support of Safety Emporium.

About This Archive \|	DCHAS-L 2020 Index \|	DCHAS-L Yearly Index
Search All Posts: Advanced Search Disclaimer

Interactive Learning Paradigms, Incorporated

DCHAS-L Discussion List Archive