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Subject: [DCHAS-L] Lab Hydrogenation

Date: Oct 1, 2024 16:31 UTC

Author: Galdenzi, Bill <bill.galdenzi**At_Symbol_Here**ALEXION.COM>

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Subject: Re: [DCHAS-L] Lab Hydrogenation

Date: Oct 2, 2024 00:02 UTC

Author: Matthew Meredith <matthewmeredith34**At_Symbol_Here**GMAIL.COM>

From: Kari Kramp <KKramp**At_Symbol_Here**LOYALISTCOLLEGE.COM>

Subject: Re: [DCHAS-L] Lab Hydrogenation

Date: Oct 1, 2024 23:21 UTC

Reply-To: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**Princeton.EDU>

Message-ID: <YT3P288MB0157DA4A276A00ED325F0CF8C9772**At_Symbol_Here**YT3P288MB0157.CANP288.PROD.OUTLOOK.COM>

In-Reply-To: <PR3PR04MB7258142C0F07F7C223B563A9FE772**At_Symbol_Here**PR3PR04MB7258.eurprd04.prod.outlook.com>

Demystify: 
https://chem.wisc.edu/wp-content/uploads/sites/1130/2019/12/JCHAS-2016-tc2.pdf
I only have experience with the balloon method but found this article. :)

From: ACS Division of Chemical Health and Safety <DCHAS-L**At_Symbol_Here**Princeton.EDU> on behalf of Galdenzi, Bill <bill.galdenzi**At_Symbol_Here**ALEXION.COM>
Sent: Tuesday, October 1, 2024 12:31:42 PM
To: DCHAS-L**At_Symbol_Here**Princeton.EDU <DCHAS-L**At_Symbol_Here**Princeton.EDU>
Subject: [DCHAS-L] Lab Hydrogenation
 
You don't often get email from bill.galdenzi@alexion.com. Learn why this is important

Dear CHAS members

 

Wondered if anyone has some experience and specific guidance on lab hydrogenations specific to a Parr unit designed for lab scale hydrogenations:

 

  1. Scale limitations (pressure and volumes) for lab.
  2. Does it vary by floor?
  3. Special considerations – hydrogen monitor
  4. Limitations to cylinders
  5. Hood construction (hood sash considerations)
  6. Other??

 

Any procedures, SOP, slide decks….etc. would be greatly appreciated.    Thank you

 

Bill Galdenzi

Environmental, Health and Safety

Cell = (475) 331-1698

email       bill.galdenzi**At_Symbol_Here**alexion.com

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